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You should first stop should be in Reliance where you can leave one or more vehicles at the Webb General Store. The Webb store is easy to find, as it is the only thing in Reliance and sits at the junction of Highway 30 and the Hiwassee River. You can also rent inner tubes and also inflatable type kayaks. There is a truck that makes regular runs up river during the day carrying passengers and tubes up the river to the dam. If you were by yourself, you it may be possible hitch a ride for you and a kayak, but we always used a second vehicle to transport ourselves up one of the several parking areas close to the dam.
The Kayak Wing
PFD's (Life Jackets)
Hardshell Kayak Sail Rigs